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Synthesis of LiCoO2 Nanoparticles by a Sonochemical Method under the Multibubble Sonoluminescence Conditions
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  • Synthesis of LiCoO2 Nanoparticles by a Sonochemical Method under the Multibubble Sonoluminescence Conditions
  • Synthesis of LiCoO2 Nanoparticles by a Sonochemical Method under the Multibubble Sonoluminescence Conditions
저자명
Park. Jong-Pil,Park. Jea-Young,Hwang. Cha-Hwan,Choi. Myung-Ho,Kim. Jee-Eon,Ok. Kang-Min,Shim. Il-Wun
간행물명
Bulletin of the Korean Chemical Society
권/호정보
2010년|31권 2호|pp.327-330 (4 pages)
발행정보
대한화학회
파일정보
정기간행물|ENG|
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기타
이 논문은 한국과학기술정보연구원과 논문 연계를 통해 무료로 제공되는 원문입니다.
서지반출

기타언어초록

$LiCoO_2$, a cathode material for lithium rechargeable batteries, was prepared in a nanoscale through a simple sonochemistry. First, $Co_3O_4$ nanoparticles were prepared by reacting NaOH and $CoCl_2$ or $CoSO_4$ with a sonochemical method, operated at 20 kHz and 220 W for 20 min, very powerful multibubble sonoluminescence conditions for chemical reactions. Second, LiOH was coated onto the $Co_3O_4$ nanoparticles by the same method as above. Finally, $LiCoO_2$ nanoparticles of about 10~30 nm size in diameter were obtained by the thermal treatment of the resulting LiOH-coated $Co_3O_4$ nanoparticles at $500^{circ}C$ for 3 hr. This synthetic process is relatively quite mild and simple compared to the known method for the synthesis of $LiCoO_2$ nanoparticles. The materials synthesized were characterized by infrared spectroscopy, X-ray diffraction, inductively coupled plasma spectrometer, and high resolution-transmission electron microscopy analyses.