- 축산식품 중 비스테로이드성 항염증 약물의 잔류함량 모니터링
- ㆍ 저자명
- 최윤화,김연주,신방우,이정학,Choi. Yoon-Hwa,Kim. Yoen-Joo,Shin. Bang-Woo,Lee. Jung-Hark
- ㆍ 간행물명
- 韓國家畜衛生學會誌
- ㆍ 권/호정보
- 2011년|34권 3호|pp.285-289 (5 pages)
- ㆍ 발행정보
- 한국가축위생학회
- ㆍ 파일정보
- 정기간행물| PDF텍스트
- ㆍ 주제분야
- 기타
This study was conducted to determine the content of non-steroidal anti-inflammatory drugs (NSAIDs) in meats available on the Korean markets. The analysis was carried out using following conditions; C18 column ($100{ imes}2.1$ mm, 1.7 ${mu}m$), mobile phase composed of DW (containing 0.1% formic acid): acetonitrile (containing 0.1% formic acid), binary pump at a flow rate of 0.3 ml/min and 5 ${mu}l$ of injection volume, MS/MS detector with ESI positive mode. The calibration range of five NSAIDs showed linearity ($r^2{geq}0.99$) at concentration range of 3.125~200 ${mu}g$/kg. The recoveries in fortified muscle more than 78.7~100.3%. The detection limits for meloxicam, ketoprofen, flunixin, carprofen and tolfenamic acid were 3.5, 1.6, 1.7, 9.8 and 4.8 ${mu}g$/kg, respectively. We also monitored NSAIDs residue in cattle muscle 51 samples. The test results, NSAIDs were all not founded.