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포름알데히드로 세리신 정착 후 정련에 의한 실크 생사의 반숙 정련
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  • 포름알데히드로 세리신 정착 후 정련에 의한 실크 생사의 반숙 정련
저자명
박건용,박창혁,정화진,이미연,이정주,박두경,Park. Geon Yong,Park. Chang Hyouck,Jeong. Hwa Jin,Lee. Mi Yeon,Lee. Jung Ju,Park. Du Keong
간행물명
韓國纖維工學會誌
권/호정보
2012년|49권 5호|pp.301-306 (6 pages)
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한국섬유공학회
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이 논문은 한국과학기술정보연구원과 논문 연계를 통해 무료로 제공되는 원문입니다.
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기타언어초록

To obtain the half-degummed silk yarns of 5~10% degumming losses, raw silk yarns were degummed with alkaline detergent after fixing sericin with formaldehyde. Adding above 5 g/l acetic acid or tartaric acid in 1% and 5% formaldehyde fixing baths created a lot of sericin loss during degumming with 3 g/l alkaline detergent and 2 g/l sodium carbonate after fixing sericin due to alkaline hydrolysis of sericin cross-linkage. When sericin was degummed with 3 g/l alkaline detergent after fixing with 0.1% formaldehyde at $40^{circ}C$ or $60^{circ}C$ for 15 min, the degumming temperature necessary to obtain satisfactory half-degumming was $70{sim}80^{circ}C$. Also, fixing sericin at $60^{circ}C$ resulted in stronger sericin fixation than fixing at $40^{circ}C$. However, the softener of cationic surfactant added in sericin fixing baths did not prevent the attachment of degummed silk yarns. Approximately 6.5% degumming loss was obtained when sericin was degummed at $85^{circ}C$ for 30 min with 3 g/l alkaline detergent after fixing with 0.1% formaldehyde at $80^{circ}C$ for 15 min and 30 min, and in case of adding 2 g/l acetic acid in fixing baths the half-degummed silk yarns of about 10% degumming losses, which were severely attached to each other, were obtained.