- 함침법에 의한 지르코니아 나노 분말의 합성
- ㆍ 저자명
- 한정화,김수종,Han. Cheong-Hwa,Kim. Soo-Jong
- ㆍ 간행물명
- 한국세라믹학회지
- ㆍ 권/호정보
- 2012년|49권 5호|pp.454-460 (7 pages)
- ㆍ 발행정보
- 한국세라믹학회
- ㆍ 파일정보
- 정기간행물| PDF텍스트
- ㆍ 주제분야
- 기타
The nano-sized zirconia powders were synthesized in an impregnation method using pulp and $ZrOCl_2{cdot}8H_2O$ as an initial material. The synthesized powders were characterized by XRD and FE-SEM. The particle size of the powder was controlled by preparation conditions, such as drying temperature and time. As a result of the various drying and calcination conditions, 30~50 nm sized homogeneous zirconia particles were obtained at $800^{circ}C$ for 1 h. Crystallization and the rapid growth of particles were accelerated with increasing calcination temperature and time. Tetragonal phase generated below $800^{circ}C$ were transferred to monoclinic phase with increasing calcination temperature and time. Moreover, above $800^{circ}C$, heat treatment time had very large influence on the particle growth, and the change of drying condition also had large influence on the growth of a crystal.