- 돼지고기에서 7종 mycotoxins 잔류실태 조사
- ㆍ 저자명
- 김연주,김미란,최태석,김영섭,이주형,Kim. Yoen-Joo,Kim. Mi-Ran,Choi. Tae-Suk,Kim. Young-Seob,Lee. Ju-Hyoung
- ㆍ 간행물명
- 韓國家畜衛生學會誌
- ㆍ 권/호정보
- 2013년|36권 4호|pp.303-309 (7 pages)
- ㆍ 발행정보
- 한국가축위생학회
- ㆍ 파일정보
- 정기간행물| PDF텍스트
- ㆍ 주제분야
- 기타
This study was conducted to determine the content of 7 mycotoxins (aflatoxin $B_1$, $B_2$, $G_1$, $G_2$, $M_1$, ochratoxin A and zearalenone) using LC-MS/MS in pork available on the Korean markets. The analysis was carried out using following conditions; C18 column ($2.1{ imes}100mm$, $1.7{mu}m$), mobile phase composed of $H_2O$ (0.1 mM $NH_4Ac$ 0.01% HCOOH) : Methanol (0.1 mM $NH_4Ac$ 0.01% HCOOH), binary pump at a flow rate of 0.5 mL/min and $2{mu}L$ of injection volume, MS/MS detector with ESI positive and negative mode. The quantication of mycotoxins was based on matrix-matched calibration curves with a correlation coefficient in excess of 0.99 for the 7 mycotoxins. The dectection limits were ranged 0.74~2.13 ng/g, with mean recoveries between 73.10~97.46% except aflatoxin $B_1$ (61.31%). We also monitored mycotoxin residues in 208 pork samples. The test results, mycotoxins were not found except one sample. Ochratoxin A in one sample of the test samples was detected below the quantification limit.