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Grade II 순수 타이타늄의 단시간 양극산화에 의한 TiO2 나노튜브 형성
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  • Grade II 순수 타이타늄의 단시간 양극산화에 의한 TiO2 나노튜브 형성
저자명
이광민,김용재,강경호,윤두현,노상현,강석일,유대흥,임현필,윤귀덕,박상원,김현승,Lee. Kwangmin,Kim. Yongjae,Kang. Kyungho,Yoon. Duhyeon,Rho. Sanghyun,Kang. Seokil,Yo
간행물명
한국재료학회지
권/호정보
2013년|23권 4호|pp.240-245 (6 pages)
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한국재료학회
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정기간행물|
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이 논문은 한국과학기술정보연구원과 논문 연계를 통해 무료로 제공되는 원문입니다.
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기타언어초록

Electrochemical surface treatment is commonly used to form a thin, rough, and porous oxidation layer on the surface of titanium. The purpose of this study was to investigate the formation of nanotubular titanium oxide arrays during short anodization processing. The specimen used in this study was 99.9% pure cp-Ti (ASTM Grade II) in the form of a disc with diameter of 15 mm and a thickness of 1 mm. A DC power supplier was used with the anodizing apparatus, and the titanium specimen and the platinum plate ($3mm{ imes}4mm{ imes}0.1mm$) were connected to an anode and cathode, respectively. The progressive formation of $TiO_2$ nanotubes was observed with FE-SEM (Field Emission Scanning Electron Microscopy). Highly ordered $TiO_2$ nanotubes were formed at a potential of 20 V in a solution of 1M $H_3PO_4$ + 1.5 wt.% HF for 10 minutes, corresponding with steady state processing. The diameters and the closed ends of $TiO_2$ nanotubes measured at a value of 50 cumulative percent were 100 nm and 120 nm, respectively. The $TiO_2$ nanotubes had lengths of 500 nm. As the anodization processing reached 10 minutes, the frequency distribution for the diameters and the closed ends of the $TiO_2$ nanotubes was gradually reduced. Short anodization processing for $TiO_2$ nanotubes of within 10 minutes was established.