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Effects of SPS Mold on the Properties of Sintered and Simulated SiC-ZrB2 Composites
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  • Effects of SPS Mold on the Properties of Sintered and Simulated SiC-ZrB2 Composites
  • Effects of SPS Mold on the Properties of Sintered and Simulated SiC-ZrB2 Composites
저자명
Lee. Jung-Hoon,Kim. In-Yong,Kang. Myeong-Kyun,Jeon. Jun-Soo,Lee. Seung-Hoon,Jeon. An-Gyun,Shin. Yong-Deok
간행물명
Journal of electrical engineering & technology
권/호정보
2013년|8권 6호|pp.1474-1480 (7 pages)
발행정보
대한전기학회
파일정보
정기간행물|ENG|
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이 논문은 한국과학기술정보연구원과 논문 연계를 통해 무료로 제공되는 원문입니다.
서지반출

기타언어초록

Silicon carbide (SiC)-zirconium diboride ($ZrB_2$) composites were prepared by subjecting a 60:40 vol% mixture of ${eta}$-SiC powder and $ZrB_2$ matrix to spark plasma sintering (SPS) in 15 $mm{Phi}$ and 20 $mm{Phi}$ molds. The 15 $mm{Phi}$ and 20 $mm{Phi}$ compacts were sintered for 60 sec at $1500^{circ}C$ under a uniaxial pressure of 50 MPa and argon atmosphere. Similar composites were simulated using $Flux^{(R)}$ 3D computer simulation software. The current and power densities of the specimen sections of the simulated SiC-$ZrB_2$ composites were higher than those of the mold sections of the 15 $mm{Phi}$ and 20 $mm{Phi}$ mold simulated specimens. Toward the centers of the specimen sections, the current densities in the simulated SiC-$ZrB_2$ composites increased. The power density patterns of the specimen sections of the simulated SiC-$ZrB_2$ composites were nearly identical to their current density patterns. The current densities of the 15 $mm{Phi}$ mold of the simulated SiC-$ZrB_2$ composites were higher than those of the 20 $mm{Phi}$ mold in the center of the specimen section. The volume electrical resistivity of the simulated SiC-$ZrB_2$ composite was about 7.72 times lower than those of the graphite mold and the punch section. The power density, 1.4604 $GW/m^3$, of the 15 $mm{Phi}$ mold of the simulated SiC-$ZrB_2$ composite was higher than that of the 20 $mm{Phi}$ mold, 1.3832 $GW/m^3$. The $ZrB_2$ distributions in the 20 $mm{Phi}$ mold in the sintered SiC-$ZrB_2$ composites were more uniform than those of the 15 $mm{Phi}$ mold on the basis of energy-dispersive spectroscopy (EDS) mapping. The volume electrical resistivity of the 20 $mm{Phi}$ mold of the sintered SiC-$ZrB_2$ composite, $6.17{ imes}10^{-4}{Omega}cm$, was lower than that of the 15 $mm{Phi}$ mold, $9.37{ imes}10^{-4}{Omega}{cdot}cm$, at room temperature.