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Production of Porous Metallic Glass Granule by Optimizing Chemical Processing
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  • Production of Porous Metallic Glass Granule by Optimizing Chemical Processing
  • Production of Porous Metallic Glass Granule by Optimizing Chemical Processing
저자명
Kim. Song-Yi,Guem. Bo-Kyung,Lee. Min-Ha,Kim. Taek-Soo,Eckert. Jurgen,Kim. Bum-Sung
간행물명
한국분말야금학회지
권/호정보
2014년|21권 4호|pp.251-255 (5 pages)
발행정보
한국분말야금학회
파일정보
정기간행물|ENG|
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이 논문은 한국과학기술정보연구원과 논문 연계를 통해 무료로 제공되는 원문입니다.
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기타언어초록

In this study, we optimized dissolution the dissolution conditions of porous amorphous powder to have high specific surface area. Porous metallic glass(MG) granules were fabricated by selective phase dissolution, in which brass is removed from a composite powder consisting of MG and 40 vol.% brass. Dissolution was achieved through various concentrations of $H_2SO_4$ and $HNO_3$, with $HNO_3$ proving to have the faster reaction kinetics. Porous powders were analyzed by differential scanning calorimetry to observe crystallization behavior. The Microstructure of milled powder and dissolved powder was analyzed by scanning electron microscope. To check for residual in the dissolved powder after dissolution, energy dispersive X-ray spectroscory and elemental mapping was conducted. It was confirmed that the MG/brass composite powder dissolved in 10% $HNO_3$ produced a porous MG granule with a relatively high specific surface area of $19.60m^2/g$. This proved to be the optimum dissolution condition in which both a porous internal granule structure and amorphous phase were maintained. Consequently, porous MG granules were effectively fabricated and applications of such structures can be expanded.