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Improvement of gas sensing properties of carbon nanofibers based on polyacrylonitrile and pitch by steam activation
Jeongsik Kim, Hyung-Il Kim, Jumi Yun 한국탄소학회 Carbon Letters 5 Pages
한국탄소학회 Carbon Letters 2017, Vol.24 5 36-40 (5 pages)
Polyacrylonitrile/pitch nanofibers were prepared by electrospinning as a precursor for a gas sensor material. Pitch nanofibers were properly fabricated by incorporating polyacrylonitrile as an electrospinning supplement component. Polyacrylonitrile/pitch nanofibers were activated with steam at various temperatures followed by subsequent carbonization to make carbon nanofibers with a highly conductive graphitic structure. Steam activation was effective in facilitating gas adsorption onto the... -
Catalytic hydrogenation-assisted preparation of melt spinnable pitches from petroleum residue for making mesophase pitch based carbon fibers
Dong Hun Lee, Jisu Choi, Young Se Oh, Yoong Ahm Kim, Kap Seung Yang, Ho Jin Ryu, Yong Jung Kim 한국탄소학회 Carbon Letters 8 Pages
한국탄소학회 Carbon Letters 2017, Vol.24 4 28-35 (8 pages)
We demonstrated an effective way of preparing melt spinnable mesophase pitches via catalytic hydrogenation of petroleum residue (fluidized catalytic cracking-decant oil) and their subsequent thermal soaking. The mesophase pitches thus obtained were analyzed in terms of their viscosity, elemental composition, solubility, molecular weight, softening point and optical texture. We found that zeolite-induced catalytic hydrogenation under high hydrogen pressure contributed to a large variation in the... -
Effect of the surface modification using MWCNTs with different L/D by two different methods of deposition on the IFSS of single carbon fiber-epoxy resin composite
Minerva L. Herrera-Sosa, Alex Valadez-Gonz?lez, Humberto V?zquez-Torres, Pierre G. Mani-Gonz?lez, Pedro J. Herrera-Franco 한국탄소학회 Carbon Letters 10 Pages
한국탄소학회 Carbon Letters 2017, Vol.24 3 18-27 (10 pages)
Multiwall carbon nanotubes (MWCNT) with two different (L/D) aspect ratios (7±2 μm/140±30 nm and 0.5?2 μm/8?15 nm) were surface treated using nitric acid (HNO3) and polyethyleneimine (PEI) prior to their deposition on carbon fibers (CF). Before the hierarchical reinforcement with CF-MWCNT, the CFs were treated with 3-glycidoxypropyltrimethoxysilane, a coupling agent (Z6040) and with poly(amidoamine) (PAMAM) a dendrimer containing an ethylenediamine core and amine surface groups. The MWCNT... -
Effect of added mesophase pitch during the pitch synthesis reaction of PFO
Ji Hong Kim, Jong Gu Kim, Chul Wee Lee, Ki Bong Lee, Ji Sun Im 한국탄소학회 Carbon Letters 7 Pages
한국탄소학회 Carbon Letters 2017, Vol.23 7 48-54 (7 pages)
This research considers the effect of added mesophase pitch (MP) as an additive during the pitch synthesis reaction of pyrolyzed fuel oil (PFO). Two effects are generated by adding MP. One is an enhancement of thermal stability due to the high thermal property of the additive; the other is that the volatile compounds that were removed by vaporization of PFO during the thermal reaction can participate in the pitch synthesis reaction (PFO→pitch) more efficiently. The effect differs according to... -
Mechanical and electrical properties of cement paste incorporated with pitch-based carbon fiber
Inkyu Rhee, Jin Hee Kim, Sang Hee Park, Sungho Lee, Bong Ryeul Ryu, Yoong Ahm Kim 한국탄소학회 Carbon Letters 8 Pages
한국탄소학회 Carbon Letters 2017, Vol.23 4 22-29 (8 pages)
The compressive strength and electrical resistance of pitch-based carbon fiber (CF) in cementitious materials are explored to determine the feasibility of its use as a functional material in construction. The most widely used CFs are manufactured from polyacrylonitrile (PAN-based CF). Alternatively, short CFs are obtained in an economical way using pitch as a precursor in a melt-blown process (pitch-based CF), which is cheaper and more eco-friendly method because this pitch-based CF is basically... -
Effects of maleic anhydride content on mechanical properties of carbon fibers-reinforced maleic anhydride-grafted-polypropylene matrix composites
Hyun-Il Kim, Woong Han, Woong-Ki Choi, Soo-Jin Park, Kay-Hyeok An, Byung-Joo Kim 한국탄소학회 Carbon Letters 8 Pages
한국탄소학회 Carbon Letters 2016, Vol.20 6 39-46 (8 pages)
applied to increase the interfacial strength between the CFs and MAPP matrix. The mechanical properties of the CFs/MAPP composites are likely to be different in terms of MA content. Surface characteristics were observed by scanning electron microscope, Fourier transform infrared spectroscopy, and single fiber contact angle method. The mechanical properties of the composites were also measured by a critical stress intensity factor (KIC). From the KIC test results, the KIC values were increased to... -
The effect of the spinning conditions on the structure of mesophase pitch-based carbon fibers by Taguchi method
Zhao Jiang, Ting Ouyang, Xiangdong Yao, Youqing Fei 한국탄소학회 Carbon Letters 10 Pages
한국탄소학회 Carbon Letters 2016, Vol.19 11 89-98 (10 pages)
Taguchi’s experimental design was employed in the melt spinning of molten mesophase pitch to produce carbon fibers. The textures of the obtained carbon fibers were radial with varied crack angles, as observed by scanning electron microscopy and polarized optical imaging. The diameter, crack angle, preferred orientation, and tensile modulus of the produced samples were examined to investigate the influence of four spinning variables. The relative importance of the variables has been emphasized... -
Pitch-based carbon fibers from coal tar or petroleum residue under the same processing condition
Jiyoung Kim, Ui-Su Im, Byungrok Lee, Dong-Hyun Peck, Seong-Ho Yoon, Doo-Hwan Jung 한국탄소학회 Carbon Letters 7 Pages
한국탄소학회 Carbon Letters 2016, Vol.19 9 72-78 (7 pages)
Spinnable pitches and carbon fibers were successfully prepared from petroleum or coal pyrolysis residues. After pyrolysis fuel oil (PFO), slurry oil, and coal tar were simply filtered to eliminate the solid impurities, the characteristics of the raw materials were evaluated by elemental analysis, 13C nuclear magnetic resonance spectrometer, matrix-assisted laser desorption/ionization time-of-flight mass spectrometer (MALDI-TOF-MS), and so on. Spinnable pitches were prepared for melt-spinning...
