- 내구유연발수제에 관한 연구(제4보) -1,2-이치환 이미다졸린-요소 축합물의 합성-
- ㆍ 저자명
- 심정변,박홍수홍성일
- ㆍ 간행물명
- 韓國纖維工學會誌
- ㆍ 권/호정보
- 1976년|13권 3호|pp.18-27 (10 pages)
- ㆍ 발행정보
- 한국섬유공학회
- ㆍ 파일정보
- 정기간행물| PDF텍스트
- ㆍ 주제분야
- 기타
Two moles of 1-stearoyl aminoethy1-2-heptadecylimidazoline(SHI), 1-stearoyl bis (aminoethyl)-2-heptadecyl imidazoline (SDI) or 1-stearoyl tris (aminoethyl)-2-heptadecyl imidazoline (STI) reacted with one mole to three moles of urea to form one mole of 1,2-disubstituted imidazolineurea condensate such as SHI-urea (SHIU), SDI-urea (SDIU) or STI-urea (STIU) by condensation in reaction much like that of 1,3-distearoy1-6, 8-bis (2-hydroxyethyl)-1,3,6,8-tetraaza cyclodecane-2, 7-dione (DDTC), which has been synthesized as the model compound prior to the dimerization. SHIU, SDIU and STIU were characaterized by means of IR spectroscopy, elemental analysis and molecular weight measurement. Quaternized SHIU (SHIUC), SDIU (SDIUC) and STIU (STIUC) were formed by combination of SHIU, SDIU and STIU with epchlorohydrin, respectively, and the hydrated to produce SHIUCW and STIUCW.