- 생약 중 잔류농약의 분석(I) - GC에 의한 16종의 잔류 규제 농약의 분석 -
- ㆍ 저자명
- 박만기,박정일,윤혜란,이은정,이수연,노일협
- ㆍ 간행물명
- 약학회지
- ㆍ 권/호정보
- 1993년|37권 1호|pp.54-65 (12 pages)
- ㆍ 발행정보
- 대한약학회
- ㆍ 파일정보
- 정기간행물| PDF텍스트
- ㆍ 주제분야
- 기타
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A method for the determination of 16 residual pesticides in crude deugs was examined. Crude drug was extracted with acetonitrile/water solution and the extract was partitioned between hexane/CH$_{2}$Cl$_{2}$ and NaCl saturated water. The organic layer was passed through cleanup column and subjected to the GC/ECD or GC/NPD analysis. Essential oil components in crude drug interfere with the analysis, and sulfuric acid treatment was adapted to overcome this interference.