- SHS화학로에 의한 SiC의 합성
- ㆍ 저자명
- 김도경,박성,조건,이형복
- ㆍ 간행물명
- 요업학회지
- ㆍ 권/호정보
- 1994년|31권 11호|pp.1283-1292 (10 pages)
- ㆍ 발행정보
- 한국세라믹학회
- ㆍ 파일정보
- 정기간행물| PDF텍스트
- ㆍ 주제분야
- 기타
Ultra-fine $eta$-SiC powders were fabricated by self-propagating high temperature synthesis process (SHS) using chemical furnace. The dependences of the C powders with different surface areas, the molar ratios of C/Si, the weight ratios of chemical fuel content, and pellet diameter-size on synthesis were investigated. Compositional and structural characterization of these powders was carried out by scanning electron micrograph and X-ray diffraction. The $eta$-SiC powders which had C/Si mole ratio=1.05, 3 times chemical fuel contents, and pellet diameter=20 mm were optimum for synthesis efficiency. By optimizing process-variables, it is possible to fabricate $eta$-SiC powders which have little secondary phases ($alpha$-SiC).