The utilization of resonance should be considered to get the maximum effect of ultrasonic to atomize liquid. The ultrasonic generator, transducer, horn, and all attached parts are used to produce the resonance, and specially the characteristics of liquids such as liquid load, property, and etc., for the liquid atomization affinity are considered. In this study, the variable device of liquid load was made and distilled water and city water selected as experimental liquids were sprayed by a twin-fluid spray method and their diameters, distributions, and spray quantum of spray droplets were measured by the light scattering system. And all data were observed, compared and considered relatively. In results, a lot of phenomena of liquid atomization affinity by ultrasonic appeared in accordance with liquid loads, namely head h.