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Preparation of Ni Nanoparticles-TiO2 Nanotube Arrays Composite and Its Application for Electrochemical Capacitor
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  • Preparation of Ni Nanoparticles-TiO2 Nanotube Arrays Composite and Its Application for Electrochemical Capacitor
  • Preparation of Ni Nanoparticles-TiO2 Nanotube Arrays Composite and Its Application for Electrochemical Capacitor
저자명
He. Huichao,Zhang. Yunhuai,Xiao. Peng,Yang. Yannan,Lou. Qing,Yang. Fei
간행물명
Bulletin of the Korean Chemical Society
권/호정보
2012년|33권 5호|pp.1613-1616 (4 pages)
발행정보
대한화학회
파일정보
정기간행물|ENG|
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이 논문은 한국과학기술정보연구원과 논문 연계를 통해 무료로 제공되는 원문입니다.
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기타언어초록

Ni nanoparticles-$TiO_2$ nanotube arrays (Ni/$TiO_2NTs$) composites were prepared by pulsed electrodeposition method and subsequently characterized by means of field emission scanning electron microscopy (FESEM), X-ray diffraction (XRD) and energy dispersive X-ray spectroscopy (EDX). The FESEM results showed that highly dispersed Ni nanoparticles were not only loaded on the top of the $TiO_2NTs$ but also within the tubular structure, and the particle size of Ni prepared at different current amplitude (100, 200 and 300 $mA{cdot}cm^{-2}$) was in the range of 15 to 70 nm. The electrochemical studies indicated that Ni nanoparticles loaded on the highly ordered $TiO_2NTs$ are readily accessible for electrochemical reactions, which improve the efficiency of the Ni nanoparticles and $TiO_2NTs$. A maximum specific capacitance (27.3 $mF.cm^{-2}$) was obtained on the Ni/$TiO_2NTs$ composite electrode that prepared at a current of 200 $mA.cm^{-2}$, and the electrode also exhibited excellent electrochemical stability.